methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

Base Information

Chemical Name:methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate
CAS No.:1351956-92-7
Molecular Formula:C₂₄H₂₅N₃O₂S
Molecular Weight:419.547
Hs Code.:

Synonyms:methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

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Chemical Property of methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

Chemical Property:

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Technology Process of methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

There total 8 articles about methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351956-91-6
2-bromo-6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazole

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1351956-92-7
methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 80 ℃; for 6h; Inert atmosphere;

Reference yield:

: N-(4-(2-ethyl-1-hydroxybutyl)phenyl)acetamide

: 1351956-92-7
methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetonitrile / 20 °C

2.1: hydrogenchloride / water / 60 °C

2.2: pH 12 - 14 / Cooling with ice

3.1: bromine / acetic acid

3.2: pH 12 / Cooling with ice

4.1: copper(ll) bromide; sodium nitrite; hydrogen bromide / acetonitrile; water / 2.5 h / -10 - 20 °C

5.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 6 h / 80 °C / Inert atmosphere

With hydrogenchloride; hydrogen bromide; bromine; potassium carbonate; copper(ll) bromide; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; acetic acid; acetonitrile;

Reference yield:

: 1688-71-7
1-(4-aminophenyl)butan-1-one

: 1351956-92-7
methyl 4-(6-(2-ethyl-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)benzoate

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dmap / dichloromethane / 48 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

2.2: 20 °C

3.1: sodium tetrahydroborate / methanol / 20 °C / Cooling with ice; Inert atmosphere

4.1: acetonitrile / 20 °C

5.1: hydrogenchloride / water / 60 °C

5.2: pH 12 - 14 / Cooling with ice

6.1: bromine / acetic acid

6.2: pH 12 / Cooling with ice

7.1: copper(ll) bromide; sodium nitrite; hydrogen bromide / acetonitrile; water / 2.5 h / -10 - 20 °C

8.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 6 h / 80 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; hydrogen bromide; bromine; potassium carbonate; triethylamine; copper(ll) bromide; lithium diisopropyl amide; sodium nitrite; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; acetic acid; acetonitrile;