Technology Process of Neopentyl-(2-nitrophenyl)-sulfon
There total 5 articles about Neopentyl-(2-nitrophenyl)-sulfon which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
acetic acid;
1.) below 80 deg C, 80 min 2.) reflux, 2 h;
DOI:10.1002/hlca.19800630610
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / Pyridin / 1.) 0 deg C, 30 min 2.) 20 deg C, 3 h
2: Natriumhydrogensulfid / various solvent(s) / 3 h / 50 °C
3: 96.4 percent / KOH / dimethylformamide; H2O / 1.) between -3 and +2 deg C, 40 min, 2.) 80 deg C, 1 h
4: 88.9 percent / H2O2 / acetic acid / 1.) below 80 deg C, 80 min 2.) reflux, 2 h
With
pyridine; potassium hydroxide; sodium hydrogensulfide; dihydrogen peroxide;
In
water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19800630610
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 96.4 percent / KOH / dimethylformamide; H2O / 1.) between -3 and +2 deg C, 40 min, 2.) 80 deg C, 1 h
2: 88.9 percent / H2O2 / acetic acid / 1.) below 80 deg C, 80 min 2.) reflux, 2 h
With
potassium hydroxide; dihydrogen peroxide;
In
water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19800630610
