bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum

Base Information

Chemical Name:bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum
CAS No.:82182-11-4
Molecular Formula:C₁₃H₁₅BrMoO₃
Molecular Weight:395.104
Hs Code.:

Synonyms:bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum

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Technology Process of bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum

There total 2 articles about bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: dimer of (η(5)-pentamethylcyclopentadienyl)tricarbonylmolybdenum

: 932-87-6
1-Bromo-2-phenylacetylene

: 82182-11-4
bromo(η5-pentamethylcyclopentadienyl)tricarbonyl molybdenum

: [(η(5)-C5Me5)(CO)3Mo(σ-CCPh)]

Guidance literature:: With potassium Sodium; In tetrahydrofuran; dry Ar atmosphere; monomeric anionic intermediate obtaining from dimericcompd. and Na/K alloy in THF soln., soln. filtration, soln. of haloalky ne addn. (-110°C, stirring, -70°C, 15 min), mixture warming to room temperature during 45 min; solvent removing in vacuum, residue sepn. by column chromy. (SiO2, benzene-hexane), re-pptn. (with hexane from benzene); elem. anal.;
DOI:10.1007/BF02496023