C₂₅H₁₈FNO₇

Base Information

Chemical Name:C₂₅H₁₈FNO₇
CAS No.:1374233-78-9
Molecular Formula:C₂₅H₁₈FNO₇
Molecular Weight:463.419
Hs Code.:

C<sub>25</sub>H<sub>18</sub>FNO<sub>7</sub>

Synonyms:C₂₅H₁₈FNO₇

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Chemical Property of C₂₅H₁₈FNO₇

Chemical Property:

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Technology Process of C₂₅H₁₈FNO₇

There total 9 articles about C₂₅H₁₈FNO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₂₆FNO₇

: 1374233-78-9
C₂₅H₁₈FNO₇

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; for 1h; Reflux;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374233-78-9
C₂₅H₁₈FNO₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: boron trichloride / dichloromethane / -78 - -40 °C

7.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

8.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

9.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

With hydrogenchloride; potassium phosphate; water; nitric acid; sodium acetate; boron trichloride; sodium hydride; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374233-78-9
C₂₅H₁₈FNO₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: boron trichloride / dichloromethane / -78 - -40 °C

6.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

7.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

8.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

With hydrogenchloride; potassium phosphate; water; nitric acid; sodium acetate; boron trichloride; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;