3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

Base Information

Chemical Name:3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate
CAS No.:1037492-17-3
Molecular Formula:C₂H₂O₄*C₁₇H₁₇ClF₃NO
Molecular Weight:433.812
Hs Code.:

Synonyms:3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

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Chemical Property of 3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

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Technology Process of 3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

There total 3 articles about 3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81355-99-9
3-(4-chlorophenyl)-3-hydroxy-N-methylpropylamine

: 98-56-6
4-chlorobenzotrifluoride

: 1037492-17-3
3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

Guidance literature:: 3-(4-chlorophenyl)-3-hydroxy-N-methylpropylamine; With sodium hydride; In dimethyl sulfoxide; at 25 ℃;

4-chlorobenzotrifluoride; With potassium iodide; In dimethyl sulfoxide; at 70 ℃; for 3h;

Reference yield:

: 6286-07-3
3-(benzyl-methyl-amino)-1-(4-chloro-phenyl)-propan-1-one; hydrochloride

: 1037492-17-3
3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / methanol / 0.25 h / 15 °C

1.2: 10 °C

2.1: potassium carbonate / chloroform

3.1: potassium hydroxide; water / dimethyl sulfoxide / 4 h / 60 - 65 °C

4.1: sodium hydride / dimethyl sulfoxide / 25 °C

4.2: 3 h / 70 °C

With potassium hydroxide; sodium hydroxide; water; sodium hydride; potassium carbonate; In methanol; chloroform; dimethyl sulfoxide;

Reference yield:

: 99-91-2
para-chloroacetophenone

: 1037492-17-3
3-(4-chlorophenyl)-N-methyl-3-(4-(trifluoromethyl)phenoxy)propan-1-amine oxalate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / isopropyl alcohol / 15 °C

1.2: 7 h / Heating / reflux

2.1: sodium hydroxide / methanol / 0.25 h / 15 °C

2.2: 10 °C

3.1: potassium carbonate / chloroform

4.1: potassium hydroxide; water / dimethyl sulfoxide / 4 h / 60 - 65 °C

5.1: sodium hydride / dimethyl sulfoxide / 25 °C

5.2: 3 h / 70 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; water; sodium hydride; potassium carbonate; In methanol; chloroform; dimethyl sulfoxide; isopropyl alcohol; 1.1: Mannich Reaction;