3-[benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one

Base Information

Chemical Name:3-[benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one
CAS No.:6286-07-3
Molecular Formula:C17H18 Cl N O . Cl H
Molecular Weight:324.25
Hs Code.:

Synonyms:1-Propanone,1-(4-chlorophenyl)-3-[methyl(phenylmethyl)amino]-, hydrochloride (9CI);3-[Benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one hydrochloride; NSC 10570

Suppliers and Price of 3-[benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 3-[benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one

Chemical Property:

Vapor Pressure:5.06E-07mmHg at 25°C
Boiling Point:412.7°C at 760 mmHg
Flash Point:203.4°C
Density:1.149g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-[benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one

There total 1 articles about 3-[benzyl(methyl)amino]-1-(4-chlorophenyl)propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 99-91-2
para-chloroacetophenone

: 103-67-3
benzyl-methyl-amine

: 6286-07-3
3-(benzyl-methyl-amino)-1-(4-chloro-phenyl)-propan-1-one; hydrochloride

Guidance literature:: benzyl-methyl-amine; With hydrogenchloride; In isopropyl alcohol; at 15 ℃;

formaldehyd; para-chloroacetophenone; In isopropyl alcohol; for 7h; Heating / reflux;

Reference yield:

: 6286-07-3
3-(benzyl-methyl-amino)-1-(4-chloro-phenyl)-propan-1-one; hydrochloride

: 1037492-18-4
3-(benzyl(methyl)amino)-1-(4-chlorophenyl)propan-1-ol

Guidance literature:: 3-(benzyl-methyl-amino)-1-(4-chloro-phenyl)-propan-1-one; hydrochloride; With sodium hydroxide; In methanol; at 15 ℃; for 0.25h;

With sodium tetrahydroborate; In methanol; at 10 ℃;

With water;

Reference yield:

: 6286-07-3
3-(benzyl-methyl-amino)-1-(4-chloro-phenyl)-propan-1-one; hydrochloride

: 81355-99-9
3-(4-chlorophenyl)-3-hydroxy-N-methylpropylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol / 0.25 h / 15 °C

1.2: 10 °C

2.1: potassium carbonate / chloroform

3.1: potassium hydroxide; water / dimethyl sulfoxide / 4 h / 60 - 65 °C

With potassium hydroxide; sodium hydroxide; water; potassium carbonate; In methanol; chloroform; dimethyl sulfoxide;