2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

Base Information

Chemical Name:2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride
CAS No.:120794-46-9
Molecular Formula:C₂₅H₃₂N₄O₄*2ClH
Molecular Weight:525.475
Hs Code.:

Synonyms:2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

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Chemical Property of 2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

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Technology Process of 2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

There total 5 articles about 2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 112441-27-7
2,2'-dimethoxy-4,4'-dicyano-α,ω-diphenoxypentane

: 107-15-3,85404-18-8
ethylenediamine

: 120794-46-9
2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

Guidance literature:: 2,2'-dimethoxy-4,4'-dicyano-α,ω-diphenoxypentane; With hydrogenchloride; ethanol; In 1,4-dioxane; at 0 - 20 ℃;

ethylenediamine; In ethanol; at 20 ℃; for 48h;
DOI:10.1021/jm801547t

Reference yield: 57.0%

: C₂₅H₃₄N₂O₆*2ClH

: 107-15-3,85404-18-8
ethylenediamine

: 120794-46-9
2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

Guidance literature:: In methanol; for 4h; Heating;

Reference yield:

: 28335-42-4
4-cyano-2-methoxyphenyl acetate

: 120794-46-9
2,2'-dimethoxy-4,4'-diimidazolino-α,ω-diphenoxypentane dihydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 4percent KOH / ethanol / 0.33 h / Heating

2: 1.) aq. NaOH / 1.) C₂H₅OH, reflux, 1 h, 2.) C₂H₅OH, reflux, 3 h

3: 62 percent / HCl (gas) / CHCl₃ / 168 h / Ambient temperature

4: 57 percent / methanol / 4 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydroxide; In methanol; ethanol; chloroform;