2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

Base Information

Chemical Name:2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol
CAS No.:1293294-82-2
Molecular Formula:C₁₅H₁₁F₃N₄S
Molecular Weight:336.34
Hs Code.:

Synonyms:2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

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Chemical Property of 2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

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Technology Process of 2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

There total 6 articles about 2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1293294-91-3
2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzene-1-sulfonyl chloride

: 1293294-82-2
2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

Guidance literature:: With phosphorus; acetic acid; iodine; at 100 ℃; for 1.5h;

Reference yield:

: 637-60-5,35467-65-3
p-tolylhydrazine hydrochloride

: 1293294-82-2
2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium acetate / ethanol / 2 h / Reflux

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.1: ammonia / chloroform; water / 1.5 h / 20 °C

4.1: toluene-4-sulfonic acid / toluene / 1 h / Reflux

4.2: 20 h / 20 °C

5.1: chlorosulfonic acid / 3 h / 120 °C / Cooling with ice

6.1: phosphorus; acetic acid / iodine / 1.5 h / 100 °C

With chlorosulfonic acid; phosphorus; N-Bromosuccinimide; ammonia; sodium acetate; toluene-4-sulfonic acid; acetic acid; iodine; In ethanol; chloroform; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 524699-80-7
2,2,2-trifluoro-N'-(p-tolyl)acetohydrazonamide

: 1293294-82-2
2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / 1 h / Reflux

1.2: 20 h / 20 °C

2.1: chlorosulfonic acid / 3 h / 120 °C / Cooling with ice

3.1: phosphorus; acetic acid / iodine / 1.5 h / 100 °C

With chlorosulfonic acid; phosphorus; toluene-4-sulfonic acid; acetic acid; iodine; In toluene;