2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

Base Information

Chemical Name:2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine
CAS No.:1293293-84-1
Molecular Formula:C₁₇H₁₂F₆N₄S
Molecular Weight:418.365
Hs Code.:

Synonyms:2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

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Chemical Property of 2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

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Technology Process of 2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

There total 6 articles about 2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 353-83-3
1,1,1-trifluoro-2-iodoethane

: 1293294-82-2
2-methyl-5-(5-(pyridin-2-yl)-3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenethiol

: 1293293-84-1
2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

Guidance literature:: With rongalite; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 637-60-5,35467-65-3
p-tolylhydrazine hydrochloride

: 1293293-84-1
2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium acetate / ethanol / 2 h / Reflux

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.1: ammonia / chloroform; water / 1.5 h / 20 °C

4.1: toluene-4-sulfonic acid / toluene / 1 h / Reflux

4.2: 20 h / 20 °C

5.1: chlorosulfonic acid / 3 h / 120 °C / Cooling with ice

6.1: phosphorus; acetic acid / iodine / 1.5 h / 100 °C

7.1: potassium carbonate; rongalite / N,N-dimethyl-formamide / 16 h / 20 °C

With chlorosulfonic acid; phosphorus; N-Bromosuccinimide; ammonia; sodium acetate; rongalite; potassium carbonate; toluene-4-sulfonic acid; acetic acid; iodine; In ethanol; chloroform; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 524699-80-7
2,2,2-trifluoro-N'-(p-tolyl)acetohydrazonamide

: 1293293-84-1
2-(1-(4-methyl-3-(2,2,2-trifluoroethylthio)phenyl)-3-(trifluoromethyl)-1H-1,2,4-triazol-5-yl)pyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 1 h / Reflux

1.2: 20 h / 20 °C

2.1: chlorosulfonic acid / 3 h / 120 °C / Cooling with ice

3.1: phosphorus; acetic acid / iodine / 1.5 h / 100 °C

4.1: potassium carbonate; rongalite / N,N-dimethyl-formamide / 16 h / 20 °C

With chlorosulfonic acid; phosphorus; rongalite; potassium carbonate; toluene-4-sulfonic acid; acetic acid; iodine; In N,N-dimethyl-formamide; toluene;