[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

Base Information

Chemical Name:[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester
CAS No.:228405-25-2
Molecular Formula:C₂₄H₃₅O₅PSi
Molecular Weight:462.598
Hs Code.:

Synonyms:[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

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Chemical Property of [6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

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Technology Process of [6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

There total 3 articles about [6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 179690-97-2
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid methyl ester

: 756-79-6
dimethyl methane phosphonate

: 228405-25-2
[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran;
DOI:10.1016/S0040-4039(99)00579-1

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 228405-25-2
[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / Et₃N

2: 95 percent / imidazole / dimethylformamide

3: 94 percent / n-BuLi / tetrahydrofuran

With 1H-imidazole; n-butyllithium; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00579-1

Reference yield:

: 14273-92-8
methyl 5-hydroxypentanoate

: 228405-25-2
[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / imidazole / dimethylformamide

2: 94 percent / n-BuLi / tetrahydrofuran

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00579-1