trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester
CAS No.:862563-47-1
Molecular Formula:C₁₄H₁₈F₃NO₄S
Molecular Weight:353.362
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

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Chemical Property of trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

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Technology Process of trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

There total 4 articles about trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Trifluoro-methanesulfonic acid 3-{[(E)-furan-2-ylmethylimino]-methyl}-3-methyl-cyclohex-1-enyl ester

: 862563-47-1
trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h;
DOI:10.1021/ol051184v

Reference yield:

: 862563-59-5
trifluoromethanesulfonic acid 3-formyl-3-methyl-cyclohex-1-enyl ester

: 862563-47-1
trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; molecular sieves 3 Angstroem / methanol / 17 h / 23 °C

2: NaBH₄ / methanol / 0.5 h

With sodium tetrahydroborate; 3 A molecular sieve; triethylamine; In methanol;
DOI:10.1021/ol051184v

Reference yield:

: 862563-46-0
trifluoromethanesulfonic acid 3-cyano-3-methyl-cyclohex-1-enyl ester

: 862563-47-1
trifluoromethanesulfonic acid 3-{[(furan-2-ylmethyl)-amino]-methyl}-3-methyl-cyclohex-1-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / DIBAL-H / toluene; hexane / 0.5 h / 0 °C

2: Et₃N; molecular sieves 3 Angstroem / methanol / 17 h / 23 °C

3: NaBH₄ / methanol / 0.5 h

With sodium tetrahydroborate; 3 A molecular sieve; diisobutylaluminium hydride; triethylamine; In methanol; hexane; toluene;
DOI:10.1021/ol051184v