ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

Base Information

Chemical Name:ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate
CAS No.:154325-78-7
Molecular Formula:C₃₂H₃₇ClN₂O₃S
Molecular Weight:565.176
Hs Code.:

Synonyms:ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

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Chemical Property of ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

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Technology Process of ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

There total 5 articles about ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3099-31-8
nicotinyl chloride

: 148693-71-4
3-[1-(4-Chlorobenzyl)-3-(t-butylthio)-5-hydroxyindol-2-yl]-2,2-dimethylpropanoic acid

: 154325-78-7
ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 96h; Ambient temperature;
DOI:10.1016/S0960-894X(96)00271-5

Reference yield:

: 154325-77-6
ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-hydroxyindol-2-yl]-2,2-dimethylpropionate

: 154325-78-7
ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

Guidance literature:: With potassium carbonate; In N-methyl-acetamide; diethyl ether; hexane;

Reference yield:

: 62646-04-2
1-(4-chlorobenzyl)-1-(4-methoxyphenyl)hydrazine

: 154325-78-7
ethyl 3-[1-(4-chlorobenzyl)-3-(1,1-dimethylethylthio)-5-(pyrid-3-ylmethoxy)indol-2-yl]-2,2-dimethylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH / toluene / 96 h / Ambient temperature

2: AlCl₃ / CH₂Cl₂ / 3 h

3: K₂CO₃ / dimethylformamide / 96 h / Ambient temperature

With aluminium trichloride; potassium carbonate; acetic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0960-894X(96)00271-5