μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

Base Information

Chemical Name:μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]
CAS No.:81245-20-7
Molecular Formula:C₈₈H₁₆F₄₀Fe₂N₈O
Molecular Weight:2072.78
Hs Code.:

Synonyms:μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

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Chemical Property of μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

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Technology Process of μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

There total 8 articles about μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 211934-69-9,36965-71-6
(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III) chloride

: 81245-20-7
μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

Guidance literature:: With NaOH; In dichloromethane; the starting iron-complex is dissolved in CH2Cl2 and stirred 4 h with an equal volume of NaOH;; the org. layer is separated, washed twice with H2O, dried over Na2SO4 and chromd. over neutral Al2O3 (benzene/hexane); elem. anal.;;

Reference yield:

: iron(II) chloride monohydrate

: 25440-14-6
tetrakis(pentafluorophenyl)porphyrin

: 81245-20-7
μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.apcata.2014.04.002

Reference yield:

: 25440-14-6
tetrakis(pentafluorophenyl)porphyrin

: iron(II) chloride

: 81245-20-7
μ-oxo-bis[(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(III)]

Guidance literature:: tetrakis(pentafluorophenyl)porphyrin; iron(II) chloride; With pyridine; N,N-dimethyl-formamide; In N,N-dimethyl-formamide; for 2h; Reflux; Inert atmosphere;

air; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1002/jms.3405