ZnPc[O(CH₂CH₂O)4Me]2

Base Information

Chemical Name:ZnPc[O(CH₂CH₂O)4Me]2
CAS No.:1104908-99-7
Molecular Formula:C₅₀H₅₂N₈O₁₀Zn
Molecular Weight:990.4
Hs Code.:

ZnPc[O(CH<sub>2</sub>CH<sub>2</sub>O)4Me]2

Synonyms:ZnPc[O(CH₂CH₂O)4Me]2

Suppliers and Price of ZnPc[O(CH₂CH₂O)4Me]2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ZnPc[O(CH₂CH₂O)4Me]2

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of ZnPc[O(CH₂CH₂O)4Me]2

There total 1 articles about ZnPc[O(CH₂CH₂O)4Me]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 1104643-16-4
C₆H₂(O(CH₂CH₂O)4CH₃)2(CN)2

: 5970-45-6
zinc(II) acetate dihydrate

: 91-15-6
phthalonitrile

: 14320-04-8
zinc(II) phthalocyanine

: 1104908-99-7
ZnPc[O(CH₂CH₂O)4Me]2

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pentan-1-ol; phthalonitrile (1.0 mmol) was treated with unsubstituted phthalonitrile (9.0 mmol) and Zn-contg. compd. (2.5 mmol) in pentanol at 140-150°C for 24 h, then a small amt. of DBU was added; brief cooling; volatiles were removed under reduced pressure; residue was dissolved in CHCl3; soln. was filtered to remove ZnPc; filtrate was collected, evapd.to dryness in vac.; column chromy. (silica gel, CHCl3/CH3OH); recrystn. from THF/hexane;
DOI:10.1039/b814627f