tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane

Base Information

• Chemical Name: tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane
• CAS No.: 1013635-88-5
• Molecular Formula: C₂₅H₃₂O₄Si
• Molecular Weight: 424.612

Synonyms:tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane

Chemical Property of tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane

Chemical Property:

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Technology Process of tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane

There total 1 articles about tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyltriphenylphosphonium bromide (1779-49-3) + 5-O-(tert-butyldiphenylsilyl)-1,2-O-isopropylidene-β-D-threo-pentofuranose-3-ulose (172751-32-5) → tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane (1013635-88-5)

Guidance literature:

With n-butyllithium; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2007.12.104

Reference yield: 85.0%

tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane (1013635-88-5) → 5-O-tert-butyldiphenylsilyl-3-C-hydroxymethyl-1,2-O-isopropylidene-β-D-lyxofuranoside

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 0 - 20 ℃; for 36h;

DOI:10.1021/jo011127p

Reference yield: 76.0%

acetic anhydride (108-24-7) + tert-butyl-(2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane (1013635-88-5) → C26H32O6Si (1256086-84-6)

Guidance literature:

With sulfuric acid; acetic acid;

DOI:10.1016/j.bmcl.2010.08.071

upstream raw materials:

Methyltriphenylphosphonium bromide

5-O-(tert-butyldiphenylsilyl)-1,2-O-isopropylidene-β-D-threo-pentofuranose-3-ulose

Downstream raw materials:

C₂₅H₃₂O₄Si

C₂₅H₃₄O₄Si

C₂₆H₃₂O₆Si

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