Technology Process of C37H40O8
There total 15 articles about C37H40O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; hydrogen; triethylamine;
In
ethyl acetate;
at 20 ℃;
for 24h;
under 2250.23 Torr;
DOI:10.1055/s-0029-1217510
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetra-N-butylammonium tribromide; orthoformic acid triethyl ester / 6 h / 65 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 165 °C
3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C
4.1: acetonitrile / 6 h / Reflux
4.2: 12 h / Reflux
5.1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux
6.1: 5% Pd(II)/C(eggshell); hydrogen; triethylamine / ethyl acetate / 24 h / 20 °C / 2250.23 Torr / Autoclave
With
sodium tetrahydroborate; 18-crown-6 ether; 5% Pd(II)/C(eggshell); hydrogen; tetra-N-butylammonium tribromide; potassium carbonate; triethylamine; orthoformic acid triethyl ester;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
5.1: Wittig reaction;
DOI:10.1002/ejoc.201001023
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C
2.1: acetonitrile / 6 h / Reflux
2.2: 12 h / Reflux
3.1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux
4.1: 5% Pd(II)/C(eggshell); hydrogen; triethylamine / ethyl acetate / 24 h / 20 °C / 2250.23 Torr / Autoclave
With
sodium tetrahydroborate; 18-crown-6 ether; 5% Pd(II)/C(eggshell); hydrogen; potassium carbonate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; acetonitrile;
3.1: Wittig reaction;
DOI:10.1002/ejoc.201001023