C₃₈H₅₈O₃SeSi₂

Base Information

Chemical Name:C₃₈H₅₈O₃SeSi₂
CAS No.:1380204-60-3
Molecular Formula:C₃₈H₅₈O₃SeSi₂
Molecular Weight:698.008
Hs Code.:

C<sub>38</sub>H<sub>58</sub>O<sub>3</sub>SeSi<sub>2</sub>

Synonyms:C₃₈H₅₈O₃SeSi₂

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Chemical Property of C₃₈H₅₈O₃SeSi₂

Chemical Property:

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Technology Process of C₃₈H₅₈O₃SeSi₂

There total 13 articles about C₃₈H₅₈O₃SeSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380204-59-0
C₃₈H₅₅F₃O₆SSeSi₂

: 544-97-8
dimethyl zinc(II)

: 1380204-60-3
C₃₈H₅₈O₃SeSi₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 24h;
DOI:10.1002/anie.201201383

Reference yield:

: C₃₁H₄₈O₄Si

: 1380204-60-3
C₃₈H₅₈O₃SeSi₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / -78 °C

2.1: Hoveyda-Grubbs catalyst second generation / toluene / Reflux

3.1: N,N,N'N'-tetramethyl-1,3-propanediamine / toluene / 1 h / 0 - 20 °C

4.1: sodium tetrahydroborate / ethanol / 14 h / 0 - 20 °C

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; tert-butyl alcohol / 6.5 h / 0 - 20 °C / pH 6.6

6.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C

7.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 7 h / 0 - 20 °C

8.1: triethylamine; lithium hexamethyldisilazane / tetrahydrofuran / 3.5 h / -78 °C

9.1: palladium diacetate / dimethyl sulfoxide / 18 h / 20 °C

10.1: lithium hexamethyldisilazane / tetrahydrofuran / 22 h / -40 °C

11.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; hexane / 24 h / 0 - 20 °C

With dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Hoveyda-Grubbs catalyst second generation; N,N,N'N'-tetramethyl-1,3-propanediamine; palladium diacetate; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; hexane; dichloromethane; dimethyl sulfoxide; toluene; tert-butyl alcohol; 11.1: Negishi coupling reaction;
DOI:10.1002/anie.201201383

Reference yield:

: 1380204-48-7
C₄₃H₆₂O₇Si

: 1380204-60-3
C₃₈H₅₈O₃SeSi₂

Guidance literature:: Multi-step reaction with 10 steps

1: Hoveyda-Grubbs catalyst second generation / toluene / Reflux

2: N,N,N'N'-tetramethyl-1,3-propanediamine / toluene / 1 h / 0 - 20 °C

3: sodium tetrahydroborate / ethanol / 14 h / 0 - 20 °C

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; tert-butyl alcohol / 6.5 h / 0 - 20 °C / pH 6.6

5: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C

6: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 7 h / 0 - 20 °C

7: triethylamine; lithium hexamethyldisilazane / tetrahydrofuran / 3.5 h / -78 °C

8: palladium diacetate / dimethyl sulfoxide / 18 h / 20 °C

9: lithium hexamethyldisilazane / tetrahydrofuran / 22 h / -40 °C

10: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; hexane / 24 h / 0 - 20 °C

With dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Hoveyda-Grubbs catalyst second generation; N,N,N'N'-tetramethyl-1,3-propanediamine; palladium diacetate; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; hexane; dichloromethane; dimethyl sulfoxide; toluene; tert-butyl alcohol; 10: Negishi coupling reaction;
DOI:10.1002/anie.201201383