(R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester

Base Information

• Chemical Name: (R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester
• CAS No.: 1190373-46-6
• Molecular Formula: C₄₂H₄₅NO₁₀
• Molecular Weight: 723.82

Synonyms:(R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester

Chemical Property of (R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester

Chemical Property:

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Technology Process of (R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester

There total 1 articles about (R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + (R)-3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoic acid (1190373-45-5) → (R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester (1190373-46-6)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2009.06.016

Reference yield:

(R)-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropionic acid N-hydroxysuccinimide ester (1190373-46-6) + <2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O-((D)-ethyl-1-carbonyl)-D-glucopyranose>-L-alanyl-D-isoglutaminyl-<(L)-meso-diaminopimeloyl-(D)-amide-(L)-D-alanyl-D-alanine> → N-acetyl-β-D-glucosaminyl-(1->4)-N-acetylmuramyl-L-alanyl-D-iso-glutaminyl-{N(ε)-[(R)-3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoyl]}-meso-2,6-diaminopimelyl-D-alanyl-D-alanine

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 49h;

DOI:10.1016/j.bmc.2009.06.016

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

(R)-3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoic acid

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