Technology Process of C24H30O5
There total 13 articles about C24H30O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; boric acid;
W-2 Raney nickel;
In
methanol; water;
at 20 ℃;
for 6h;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.28 g / KF / propan-2-ol / 20 °C
2: 95 percent / methanesulfochloride; triethylamine / CH2Cl2 / 0.08 h / 0 °C
3: zinc; aq. acetic acid / tetrahydrofuran / 0.08 h / 0 °C
4: 592 mg / sodium hypochlorite / H2O; CH2Cl2 / 5 h / 20 °C
5: 85 percent / boric acid; H2 / W-2 Raney nickel / H2O; methanol / 6 h / 20 °C
With
potassium fluoride; sodium hypochlorite; hydrogen; boric acid; acetic acid; triethylamine; zinc;
W-2 Raney nickel;
In
tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: zinc; aq. acetic acid / tetrahydrofuran / 0.08 h / 0 °C
2: 592 mg / sodium hypochlorite / H2O; CH2Cl2 / 5 h / 20 °C
3: 85 percent / boric acid; H2 / W-2 Raney nickel / H2O; methanol / 6 h / 20 °C
With
sodium hypochlorite; hydrogen; boric acid; acetic acid; zinc;
W-2 Raney nickel;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol0701013