C₁₄H₆Br₂N₂S₂

Base Information

Chemical Name:C₁₄H₆Br₂N₂S₂
CAS No.:1374636-46-0
Molecular Formula:C₁₄H₆Br₂N₂S₂
Molecular Weight:426.155
Hs Code.:

C<sub>14</sub>H<sub>6</sub>Br<sub>2</sub>N<sub>2</sub>S<sub>2</sub>

Synonyms:C₁₄H₆Br₂N₂S₂

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Chemical Property of C₁₄H₆Br₂N₂S₂

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Technology Process of C₁₄H₆Br₂N₂S₂

There total 3 articles about C₁₄H₆Br₂N₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1000577-94-5
3-bromo-4-iodobenzonitrile

: 1374636-46-0
C₁₄H₆Br₂N₂S₂

Guidance literature:: 3-bromo-4-iodobenzonitrile; With TurboGrignard; at -80 ℃; Inert atmosphere;

With zinc(II) chloride; Inert atmosphere;

With disulfur dichloride; Inert atmosphere;
DOI:10.1002/anie.201106734

Reference yield:

: 50397-74-5
2-bromo-4-cyanoaniline

: 1374636-46-0
C₁₄H₆Br₂N₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; sodium nitrite / water / 2 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: TurboGrignard / -80 °C / Inert atmosphere

2.2: Inert atmosphere

2.3: Inert atmosphere

With TurboGrignard; sulfuric acid; sodium nitrite; In water;
DOI:10.1002/anie.201106734

Reference yield:

: 873-74-5
4-Aminobenzonitrile

: 1374636-46-0
C₁₄H₆Br₂N₂S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / chloroform / 3 h / 0 °C / Inert atmosphere

2.1: sulfuric acid; sodium nitrite / water / 2 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: TurboGrignard / -80 °C / Inert atmosphere

3.2: Inert atmosphere

3.3: Inert atmosphere

With N-Bromosuccinimide; TurboGrignard; sulfuric acid; sodium nitrite; In chloroform; water;
DOI:10.1002/anie.201106734