Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

Base Information

Chemical Name:Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester
CAS No.:207562-21-8
Molecular Formula:C₂₄H₂₆O₄Si
Molecular Weight:406.554
Hs Code.:

Synonyms:Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

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Chemical Property of Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

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Technology Process of Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

There total 3 articles about Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 191987-14-1
4-Bromomethyl-benzoic acid 2-trimethylsilanyl-ethyl ester

: 93-09-4
naphthalene-2-carboxylate

: 207562-21-8
Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

Guidance literature:: With potassium carbonate; In acetone; for 96h; Ambient temperature;
DOI:10.1248/cpb.46.591

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 207562-21-8
Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / N,N'-dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 18 h / Ambient temperature

2: 97 percent / K₂CO₃ / acetone / 96 h / Ambient temperature

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1248/cpb.46.591

Reference yield:

: 6232-88-8
4-bromomethylbenzoic Acid

: 207562-21-8
Naphthalene-2-carboxylic acid 4-(2-trimethylsilanyl-ethoxycarbonyl)-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / N,N'-dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 18 h / Ambient temperature

2: 97 percent / K₂CO₃ / acetone / 96 h / Ambient temperature

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1248/cpb.46.591