C₅₁H₆₆O₁₉

Base Information

Chemical Name:C₅₁H₆₆O₁₉
CAS No.:131328-67-1
Molecular Formula:C₅₁H₆₆O₁₉
Molecular Weight:983.074
Hs Code.:

C<sub>51</sub>H<sub>66</sub>O<sub>19</sub>

Synonyms:C₅₁H₆₆O₁₉

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Chemical Property of C₅₁H₆₆O₁₉

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Technology Process of C₅₁H₆₆O₁₉

There total 12 articles about C₅₁H₆₆O₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 131328-66-0
1,2,4,5-Tetra-O-benzyl-3-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

: 131328-67-1
C₅₁H₆₆O₁₉

Guidance literature:: With sodium methylate; In methanol; for 48h; Ambient temperature; pH 10;
DOI:10.1016/0008-6215(90)84051-U

Reference yield:

: 78038-31-0
Methyl 5-O-benzyl-α,β-D-ribofuranoside

: 131328-67-1
C₅₁H₆₆O₁₉

Guidance literature:: Multi-step reaction with 8 steps

1: 44 percent / 10percent aq. KOH, Bu₄NBr / CH₂Cl₂

2: 93 percent / NaH / dimethylformamide / 2 h / Ambient temperature

3: 79 percent / 1.2M HCl / dioxane / Heating

4: 85 percent / NaBH₄ / ethanol

5: 85 percent / NaH / dimethylformamide / 2 h / Ambient temperature

6: 1) t-BuOK 2) 0.1M HCl / 1) DMF, 2.5 h, 80 deg C 2) acetone, 45 min, reflux

7: 90 percent / TMS-triflate, molecular sieves (4A) / CH₂Cl₂ / 0.08 h / -30 °C

8: 98 percent / NaOMe / methanol / 48 h / Ambient temperature; pH 10

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium tert-butylate; tetrabutylammomium bromide; sodium methylate; sodium hydride; In 1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84051-U

Reference yield:

: 100-39-0
benzyl bromide

: 131328-67-1
C₅₁H₆₆O₁₉

Guidance literature:: Multi-step reaction with 8 steps

1: 44 percent / 10percent aq. KOH, Bu₄NBr / CH₂Cl₂

2: 93 percent / NaH / dimethylformamide / 2 h / Ambient temperature

3: 79 percent / 1.2M HCl / dioxane / Heating

4: 85 percent / NaBH₄ / ethanol

5: 85 percent / NaH / dimethylformamide / 2 h / Ambient temperature

6: 1) t-BuOK 2) 0.1M HCl / 1) DMF, 2.5 h, 80 deg C 2) acetone, 45 min, reflux

7: 90 percent / TMS-triflate, molecular sieves (4A) / CH₂Cl₂ / 0.08 h / -30 °C

8: 98 percent / NaOMe / methanol / 48 h / Ambient temperature; pH 10

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium tert-butylate; tetrabutylammomium bromide; sodium methylate; sodium hydride; In 1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84051-U