Technology Process of C22H24F2N4O4
There total 5 articles about C22H24F2N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / hydrogenchloride; iodine / diethyl ether / 1.5 h / 20 °C / Heating / reflux
1.2: 20 °C
2.1: boron tribromide / dichloromethane / 3 h / 0 °C
3.1: potassium carbonate / acetone / 20 °C
4.1: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 - 70 °C
With
2-hydroxypyridin; boron tribromide; potassium carbonate; magnesium; N-ethyl-N,N-diisopropylamine;
hydrogenchloride; iodine;
In
diethyl ether; dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 0.67 h / 0 °C
2: potassium carbonate / acetone / 20 °C
3: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 - 70 °C
With
pyridine; 2-hydroxypyridin; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron tribromide / dichloromethane / 3 h / 0 °C
2: potassium carbonate / acetone / 20 °C
3: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 - 70 °C
With
2-hydroxypyridin; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetone;