benzyl tert-butyl N-allyliminodicarbonate

Base Information

Chemical Name:benzyl tert-butyl N-allyliminodicarbonate
CAS No.:121561-52-2
Molecular Formula:C₁₆H₂₁NO₄
Molecular Weight:291.347
Hs Code.:

Synonyms:benzyl tert-butyl N-allyliminodicarbonate

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Chemical Property of benzyl tert-butyl N-allyliminodicarbonate

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Technology Process of benzyl tert-butyl N-allyliminodicarbonate

There total 5 articles about benzyl tert-butyl N-allyliminodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 121561-51-1
sodium benzyl tert-butyl iminodicarbonate

: 106-95-6
allyl bromide

: 121561-52-2
benzyl tert-butyl N-allyliminodicarbonate

Guidance literature:: In N,N-dimethyl-formamide; 1. -20 deg C, 30 min; 2. room temperature, 5 h;

Reference yield:

: 38091-74-6
N-(benzyloxycarbonyl)benzamide

: 121561-52-2
benzyl tert-butyl N-allyliminodicarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 3.47 g / DMAP / acetonitrile / 6 h

2: 80 percent / acetonitrile / 2 h / Ambient temperature

3: CH₃ONa / methanol / 0.17 h / -30 °C

4: 93 percent / dimethylformamide / 1. -20 deg C, 30 min; 2. room temperature, 5 h

With dmap; sodium methylate; In methanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 120542-13-4
benzyl N-[(tert-butoxy)carbonyl]carbamate

: 121561-52-2
benzyl tert-butyl N-allyliminodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃ONa / methanol / 0.17 h / -30 °C

2: 93 percent / dimethylformamide / 1. -20 deg C, 30 min; 2. room temperature, 5 h

With sodium methylate; In methanol; N,N-dimethyl-formamide;