C₁₂H₁₂INO₂

Base Information

Chemical Name:C₁₂H₁₂INO₂
CAS No.:1350557-80-0
Molecular Formula:C₁₂H₁₂INO₂
Molecular Weight:329.137
Hs Code.:

C<sub>12</sub>H<sub>12</sub>INO<sub>2</sub>

Synonyms:C₁₂H₁₂INO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₂INO₂

Chemical Property:

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Technology Process of C₁₂H₁₂INO₂

There total 4 articles about C₁₂H₁₂INO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1350557-84-4
C₁₂H₁₁BrINO₂

: 1350557-80-0
C₁₂H₁₂INO₂

Guidance literature:: With sodium tetrahydroborate; In dimethyl sulfoxide; at 20 ℃; for 0.5h;
DOI:10.1021/ja209459f

Reference yield:

: 1350557-83-3
C₁₂H₁₂INO₃

: 1350557-80-0
C₁₂H₁₂INO₂

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / acetonitrile / 0 - 20 °C

2: sodium tetrahydroborate / dimethyl sulfoxide / 0.5 h / 20 °C

With sodium tetrahydroborate; carbon tetrabromide; triphenylphosphine; In dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja209459f

Reference yield:

: C₁₄H₁₄INO₄

: 1350557-80-0
C₁₂H₁₂INO₂

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C

2: carbon tetrabromide; triphenylphosphine / acetonitrile / 0 - 20 °C

3: sodium tetrahydroborate / dimethyl sulfoxide / 0.5 h / 20 °C

With sodium tetrahydroborate; carbon tetrabromide; diisobutylaluminium hydride; triphenylphosphine; In hexane; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja209459f