benzyl 2-diazo-3-oxopentanoate

Base Information

Chemical Name:benzyl 2-diazo-3-oxopentanoate
CAS No.:86978-73-6
Molecular Formula:C₁₂H₁₂N₂O₃
Molecular Weight:232.239
Hs Code.:

Synonyms:benzyl 2-diazo-3-oxopentanoate

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Chemical Property of benzyl 2-diazo-3-oxopentanoate

Chemical Property:

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Technology Process of benzyl 2-diazo-3-oxopentanoate

There total 5 articles about benzyl 2-diazo-3-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4949-45-5
benzyl 2-methylacetoacetate

: 13407-52-8
2-naphthalenesulphonyl azide

: 86978-73-6
benzyl 2-diazo-3-oxopentanoate

Guidance literature:: With triethylamine; In acetonitrile;

Reference yield:

: 4949-45-5
benzyl 2-methylacetoacetate

: 86978-73-6
benzyl 2-diazo-3-oxopentanoate

Guidance literature:: With 4-toluenesulfonyl azide; triethylamine; In acetonitrile; at 0 - 20 ℃;
DOI:10.1016/S0040-4039(01)02386-3

Reference yield:

: 4949-44-4
ethyl propanoylacetate

: 86978-73-6
benzyl 2-diazo-3-oxopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / toluene / Heating

2: p-toluenesulfonylazide; Et₃N / acetonitrile / 0 - 20 °C

With dmap; 4-toluenesulfonyl azide; triethylamine; In toluene; acetonitrile;
DOI:10.1016/S0040-4039(01)02386-3