1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane

Base Information

• Chemical Name: 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane
• CAS No.: 1266399-81-8
• Molecular Formula: C₂₈H₃₂N₆O₄S₂
• Molecular Weight: 580.732

Synonyms:1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane

Chemical Property of 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane

Chemical Property:

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Technology Process of 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane

There total 4 articles about 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

ethyl bromoacetate (105-36-2) + C20H20N6S2 (64546-19-6) → 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane (1266399-81-8)

Guidance literature:

With potassium hydroxide; In methanol; at 0 - 20 ℃;

DOI:10.1002/jhet.729

Reference yield:

phenyl isothiocyanate (103-72-0) → 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane (1266399-81-8)

Guidance literature:

Multi-step reaction with 3 steps

1: Reflux

2: Heating; Alkaline conditions

3: acetone / Reflux

In acetone;

DOI:10.1002/ardp.201000177

Reference yield:

adipic acid dihydrazide (1071-93-8,98152-55-7) → 1,4-bis[4-phenyl-5-(carbethoxymethylmercapto)-1,2,4-triazol-3-yl]butane (1266399-81-8)

Guidance literature:

Multi-step reaction with 3 steps

1: Reflux

2: Heating; Alkaline conditions

3: acetone / Reflux

In acetone;

DOI:10.1002/ardp.201000177

upstream raw materials:

4,4'-diphenyl-1,1'-hexanedioyl-bis-thiosemicarbazide

phenyl isothiocyanate

ethyl bromoacetate

C₂₀H₂₀N₆S₂

Downstream raw materials:

1,4-bis[5-(1-oxo-1-(3,5-dimethylpyrazol-1-yl)methyl)thio-4-phenyl-1,2,4-triazol-3-yl]butane

1,4-bis-(5-[hydrazinocarbonylmethylthio]-4-phenyl-1,2,4-triazol-3-yl)butane

1,4-bis[5-(5-mercapto-1,3,4-oxadiazol-2-yl-methyl)thio-4-phenyl-1,2,4-triazol-3-yl]butane

(1⁽⁴⁾,6⁽⁴⁾-diphenyl-2,6-dithia-1,7(3,5)-1,2,4-triazola)cycloundecaphane-4-one

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