((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine

Base Information

• Chemical Name: ((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine
• CAS No.: 77495-33-1
• Molecular Formula: C₂₀H₂₉N
• Molecular Weight: 283.457

Synonyms:((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine

Chemical Property of ((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine

Chemical Property:

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Technology Process of ((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine

There total 3 articles about ((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

[(E)-5,9-Dimethyl-deca-5,9-dien-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine (77850-42-1) → (4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-((S)-1-phenyl-ethyl)-amine (77495-33-1,77495-34-2,77495-35-3,77495-36-4)

Guidance literature:

With tin(IV) chloride; In benzene;

DOI:10.1021/jo00328a023

Reference yield:

[(E)-5,9-Dimethyl-deca-5,9-dien-(E)-ylidene]-(1-phenyl-ethyl)-amine (77495-32-0,77850-42-1) → ((1S,4aR,8aR)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-35-3) + ((1R,4aR,8aR)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-34-2) + ((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-33-1) + ((1R,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-36-4)

Guidance literature:

With tin(IV) chloride; In benzene; for 24h; Yield given. Yields of byproduct given; Ambient temperature; in the dark;

DOI:10.1016/S0040-4039(00)78687-4

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + (E)-5,9-dimethyl-deca-5,9-dienal (61195-31-1) → ((1S,4aR,8aR)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-35-3) + ((1R,4aR,8aR)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-34-2) + ((1S,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-33-1) + ((1R,4aS,8aS)-4a,6-Dimethyl-1,2,3,4,4a,5,8,8a-octahydro-naphthalen-1-yl)-(1-phenyl-ethyl)-amine (77495-36-4)

Guidance literature:

With 4 A molecular sieve; tin(IV) chloride; Product distribution;

DOI:10.1021/jo00328a023

upstream raw materials:

[(E)-5,9-Dimethyl-deca-5,9-dien-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

(S)-1-phenyl-ethylamine

(E)-5,9-dimethyl-deca-5,9-dienal

[(E)-5,9-Dimethyl-deca-5,9-dien-(E)-ylidene]-(1-phenyl-ethyl)-amine

Downstream raw materials:

(S)-2-phenylbutyric acid

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