1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

Base Information

Chemical Name:1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid
CAS No.:690230-71-8
Molecular Formula:C₁₃H₂₀NO₄P
Molecular Weight:285.28
Hs Code.:

Synonyms:1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

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Chemical Property of 1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

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Technology Process of 1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

There total 3 articles about 1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.2%

: 65576-84-3
1-amino-2-methylbutylphosphinic acid

: 501-53-1,94274-21-2
benzyl chloroformate

: 690230-71-8
1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 0 - 20 ℃; pH=9 - 10;
DOI:10.1002/ardp.200600191

Reference yield:

: 96-17-3,57456-98-1
2-Methylbutyraldehyde

: 690230-71-8
1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 28.3 percent / aq. phosphinic acid / 2 h / Heating

2.1: conc. HCl / 12 h / Heating

2.2: 28.3 percent / propylene oxide / ethanol

3.1: 72.2 percent / aq. NaOH / dioxane / 0 - 20 °C / pH 9 - 10

With hydrogenchloride; sodium hydroxide; hypophosphorous acid; In 1,4-dioxane;
DOI:10.1002/ardp.200600191

Reference yield:

: 65577-20-0
1-(benzhydrylamino)-2-methylbutylphosphinic acid

: 690230-71-8
1-{[(benzyloxy)carbonyl]amino}-2-methylbutylphosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: conc. HCl / 12 h / Heating

1.2: 28.3 percent / propylene oxide / ethanol

2.1: 72.2 percent / aq. NaOH / dioxane / 0 - 20 °C / pH 9 - 10

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane;
DOI:10.1002/ardp.200600191