3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Base Information

Chemical Name:3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide
CAS No.:1383474-31-4
Molecular Formula:C₂₃H₂₂F₇N₃O₄
Molecular Weight:537.434
Hs Code.:

Synonyms:3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

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Chemical Property of 3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

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Technology Process of 3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

There total 1 articles about 3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.4%

: 107-85-7
1-amino-3-methylbutane

: 494774-76-4
2-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-4-nitro-isoindoline-1,3-dione

: 1383474-31-4
3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; regioselective reaction;
DOI:10.1002/cjoc.201100746

Reference yield: 81.7%

: 1383474-31-4
3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

: 1383474-35-8
3-amino-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 60 ℃;
DOI:10.1002/cjoc.201100746

Reference yield:

: 1383474-31-4
3-nitro-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

: 1395105-35-7
3-acetamido-N-isopentyl-N'-[2-methyl-4-(perfluoropropan-2-yl)phenyl]phthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 60 °C

2: 0.17 h / 20 °C

With palladium 10% on activated carbon; hydrogen; In methanol;
DOI:10.1002/cjoc.201100746