N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

Base Information

Chemical Name:N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide
CAS No.:1067191-56-3
Molecular Formula:C₂₂H₂₈N₂O₄
Molecular Weight:384.475
Hs Code.:

Synonyms:N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

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Chemical Property of N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

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Technology Process of N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

There total 20 articles about N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1067192-96-4
N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

: 3535-37-3
3,4-dimethoxybenzoic acid chloride

: 1067191-56-3
N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

Guidance literature:: With pyridine; at 100 ℃; for 1h; Microwave irradiation;

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 1067191-56-3
N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 8 steps

1: aluminum (III) chloride / 17.33 h / 0 - 20 °C

2: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 0 - 20 °C

3: ammonium hydroxide / dichloromethane / 1 h / 0 - 20 °C

4: sulfuric acid; potassium nitrate / dichloromethane / 16 h / 50 °C

5: borane-THF / tetrahydrofuran / 16.25 h / 80 °C

6: triethylamine / dichloromethane / 1 - 16 h / 0 - 20 °C

7: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 975.1 Torr

8: pyridine / 1 h / 100 °C / Microwave irradiation

With pyridine; aluminum (III) chloride; borane-THF; oxalyl dichloride; sulfuric acid; hydrogen; ammonium hydroxide; potassium nitrate; triethylamine; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 453562-77-1
2-methyl-2-(4-nitrophenyl)propionaldehyde

: 1067191-56-3
N-(4-(4-acetamido-2-methylbutan-2-yl)phenyl)-3,4-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.25 h / 20 °C

1.2: 2 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane; water / 1 h / 20 °C

2.2: pH 7

3.1: ammonium acetate; sodium cyanoborohydride / methanol / 20 °C

4.1: triethylamine / dichloromethane / 1 - 16 h / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 975.1 Torr

6.1: pyridine / 1 h / 100 °C / Microwave irradiation

With pyridine; ammonium acetate; hydrogen; potassium hexamethylsilazane; sodium cyanoborohydride; triethylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water;