N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

Base Information

Chemical Name:N-(3-(4-aminophenyl)-3-methylbutyl)acetamide
CAS No.:1067192-96-4
Molecular Formula:C₁₃H₂₀N₂O
Molecular Weight:220.315
Hs Code.:

Synonyms:N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

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Chemical Property of N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

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Technology Process of N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

There total 19 articles about N-(3-(4-aminophenyl)-3-methylbutyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1067192-93-1
N-[3-methyl-3-(4-nitro-phenyl)-butyl]-acetamide

: 1067192-96-4
N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 2h; under 975.098 Torr;

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 1067192-96-4
N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: aluminum (III) chloride / 17.33 h / 0 - 20 °C

2: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 0 - 20 °C

3: ammonium hydroxide / dichloromethane / 1 h / 0 - 20 °C

4: sulfuric acid; potassium nitrate / dichloromethane / 16 h / 50 °C

5: borane-THF / tetrahydrofuran / 16.25 h / 80 °C

6: triethylamine / dichloromethane / 1 - 16 h / 0 - 20 °C

7: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 975.1 Torr

With aluminum (III) chloride; borane-THF; oxalyl dichloride; sulfuric acid; hydrogen; ammonium hydroxide; potassium nitrate; triethylamine; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 453562-77-1
2-methyl-2-(4-nitrophenyl)propionaldehyde

: 1067192-96-4
N-(3-(4-aminophenyl)-3-methylbutyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.25 h / 20 °C

1.2: 2 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane; water / 1 h / 20 °C

2.2: pH 7

3.1: ammonium acetate; sodium cyanoborohydride / methanol / 20 °C

4.1: triethylamine / dichloromethane / 1 - 16 h / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 975.1 Torr

With ammonium acetate; hydrogen; potassium hexamethylsilazane; sodium cyanoborohydride; triethylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water;