6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

Base Information

Chemical Name:6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine
CAS No.:316804-48-5
Molecular Formula:C₄₂H₄₈FN₃O₁₃S₃
Molecular Weight:918.052
Hs Code.:

Synonyms:6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

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Chemical Property of 6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

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Technology Process of 6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

There total 6 articles about 6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 2466-76-4
N-Acetylimidazole

: 316804-47-4
6-O-(4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

: 316804-48-5
6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

: 6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-4-O-acetyl-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

Guidance literature:: With pyridine; In dimethyl sulfoxide; at 20 ℃; for 65h;
DOI:10.1016/S0008-6215(00)00184-1

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 316804-48-5
6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 60 °C / 35 Torr

2: 47 percent / pyridine / dimethylsulfoxide / 65 h / 20 °C

With pyridine; toluene-4-sulfonic acid; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)00184-1

Reference yield:

: 316804-46-3
6-O-(3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

: 316804-48-5
6-O-(2-O-acetyl-4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 60 °C / 35 Torr

2: 47 percent / pyridine / dimethylsulfoxide / 65 h / 20 °C

With pyridine; toluene-4-sulfonic acid; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)00184-1