3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

Base Information

Chemical Name:3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide
CAS No.:1235471-26-7
Molecular Formula:C₁₇H₁₂Cl₂N₂O₃
Molecular Weight:363.2
Hs Code.:

Synonyms:3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

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Chemical Property of 3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

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Technology Process of 3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

There total 4 articles about 3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: C₁₀H₄Cl₃NO₂

: 104-94-9
4-methoxy-aniline

: 1235471-26-7
3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

Guidance literature:: With triethylamine; In toluene; at 20 ℃; Reflux;
DOI:10.1007/s00706-010-0265-9

Reference yield:

: 378205-20-0
ethyl 3-(2,4-dichlorophenyl)isoxazole-5-carboxylate

: 1235471-26-7
3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / ethanol

2: oxalyl dichloride / benzene

3: triethylamine / toluene / 20 °C / Reflux

With oxalyl dichloride; water; triethylamine; sodium hydroxide; In ethanol; toluene; benzene;
DOI:10.1007/s00706-010-0265-9

Reference yield:

: 140946-55-0
C₁₂H₁₁Cl₂NO₃

: 1235471-26-7
3-(2,4-dichlorophenyl)isoxazole-5-carboxylic acid 4-methoxyphenylamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide

2: water; sodium hydroxide / ethanol

3: oxalyl dichloride / benzene

4: triethylamine / toluene / 20 °C / Reflux

With N-Bromosuccinimide; oxalyl dichloride; water; triethylamine; sodium hydroxide; In ethanol; toluene; benzene;
DOI:10.1007/s00706-010-0265-9