2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

Base Information

Chemical Name:2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine
CAS No.:1048034-85-0
Molecular Formula:C₁₄H₁₇ClN₄O₂S
Molecular Weight:340.834
Hs Code.:

Synonyms:2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

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Chemical Property of 2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

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Technology Process of 2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

There total 6 articles about 2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1048034-83-8
2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzonitrile

: 1048034-85-0
2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; chloroform; for 42h; under 2585.81 Torr;

Reference yield:

: 1048034-93-0
C₁₁H₂₀N₂O₂S

: 1048034-85-0
2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

1.2: 18 h / 0 - 20 °C

2.1: hydrogen / platinum(IV) oxide / ethanol; chloroform / 42 h / 2585.81 Torr

With hydrogen; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; chloroform;

Reference yield:

: 41979-39-9
4-piperidone hydrochloride

: 1048034-85-0
2-chloro-5-(5-methanesulfonyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-3-yl)-benzylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / chloroform; water / 73 h / 0 °C

2.1: toluene-4-sulfonic acid / benzene / 20 h / Heating / reflux

3.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

3.2: 18 h / 0 - 20 °C

4.1: hydrogen / platinum(IV) oxide / ethanol; chloroform / 42 h / 2585.81 Torr

With hydrogen; potassium carbonate; toluene-4-sulfonic acid; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; chloroform; water; benzene;