3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

Base Information

Chemical Name:3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester
CAS No.:87367-74-6
Molecular Formula:C₃₇H₄₈O₁₀
Molecular Weight:652.782
Hs Code.:

Synonyms:3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

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Chemical Property of 3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

There total 2 articles about 3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 87367-64-4
1,9-bis-(4'-formylphenoxy)-n-nonane

: 105-53-3
diethyl malonate

: 87367-74-6
3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

Guidance literature:: With piperidine; acetic acid; In benzene; Heating;
DOI:10.1007/BF00765771

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 87367-74-6
3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) ethanol, reflux, 4 h, 2.) reflux, 48 h

2: 89.5 percent / piperidine, glacial acetic acid / benzene / Heating

With piperidine; sodium ethanolate; acetic acid; In benzene;
DOI:10.1007/BF00765771

Reference yield:

: 87367-74-6
3-(4-{9-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-nonyloxy}-phenyl)-2-ethoxycarbonyl-acrylic acid ethyl ester

: 87367-97-3
C₂₉H₃₄N₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) NaOH / 1.) water, ethanol, heating, 2 h, 2.) ethylene glycol, heating, 40 h

2: 1.) acetic anhydride, 2.) ammonia / 1.) heating, 6 h, 2.) ethyl acetate, 2 h

3: 1 h / 200 - 220 °C

With sodium hydroxide; ammonia; acetic anhydride;
DOI:10.1007/BF00765771