C₃₂H₃₈N₄O₈S

Base Information

Chemical Name:C₃₂H₃₈N₄O₈S
CAS No.:1434648-44-8
Molecular Formula:C₃₂H₃₈N₄O₈S
Molecular Weight:638.742
Hs Code.:

C<sub>32</sub>H<sub>38</sub>N<sub>4</sub>O<sub>8</sub>S

Synonyms:C₃₂H₃₈N₄O₈S

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Chemical Property of C₃₂H₃₈N₄O₈S

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Technology Process of C₃₂H₃₈N₄O₈S

There total 14 articles about C₃₂H₃₈N₄O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1434648-38-0
C₄₈H₅₆N₄O₈SSi

: 1434648-44-8
C₃₂H₃₈N₄O₈S

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 5382-16-1
4-HYDROXYPIPERIDINE

: 1434648-44-8
C₃₂H₃₈N₄O₈S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / tetrahydrofuran / 16 h / 20 °C

2.1: triethylamine / dichloromethane / 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 110 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 1434655-18-1
tert-butyl 2-isocyanato-2-methylpropanoate

: 1434648-44-8
C₃₂H₃₈N₄O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C

1.2: 10 - 100 °C

2.1: sodium hydroxide; water / methanol / 4 h / 50 °C

3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C

4.1: bromine; CH₃COONa / acetic acid / 1 h / 20 °C

5.1: potassium carbonate / acetonitrile / 3 h / 20 °C

6.1: borane-THF / tetrahydrofuran / 8 h / 20 °C

7.1: carbon dioxide / methanol

8.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

8.2: 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 110 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With 1-methyl-pyrrolidin-2-one; tetrakis(triphenylphosphine) palladium⁽⁰⁾; borane-THF; carbon dioxide; CH₃COONa; tetrabutyl ammonium fluoride; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; acetic acid; toluene; acetonitrile;