1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

Base Information

Chemical Name:1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane
CAS No.:483356-53-2
Molecular Formula:C₃₄H₃₂N₂O₂
Molecular Weight:500.64
Hs Code.:

Synonyms:1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

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Chemical Property of 1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

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Technology Process of 1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

There total 2 articles about 1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 159152-14-4
5-(mesityl)dipyrromethane

: 63833-44-3
morpholino(p-tolyl)methanone

: 483356-53-2
1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

Guidance literature:: morpholino(p-tolyl)methanone; With trichlorophosphate; at 65 ℃; for 3h;

5-(mesityl)dipyrromethane; In 1,2-dichloro-ethane; for 2h; Heating;
DOI:10.1039/b505366h

Reference yield: 49.0%

: 874-60-2
4-methyl-benzoyl chloride

: 159152-14-4
5-(mesityl)dipyrromethane

: 483356-53-2
1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

Guidance literature:: 5-(mesityl)dipyrromethane; With ethylmagnesium bromide; In tetrahydrofuran;

4-methyl-benzoyl chloride; Further stages.;
DOI:10.1021/ol027003w

Reference yield: 17.0%

: 863413-54-1
1,1'-bis[bis-(2,2'-pyrryl)methyl]ferrocene

: 483356-53-2
1,9-bis(4-methylbenzoyl)-5-(mesityl)dipyrromethane

: 1,1'-bis[5,10-bis(4-methylphenyl)-15-mesitylporphyrin-20-yl]ferrocene

Guidance literature:: With sodium tetrahydroborate; triethylamine; trifluoroacetic acid; In acetonitrile; NaBH4 added to dipyrromethane in THF-MeOH; stirred (1 h); poured into aq. NH4Cl-CH2Cl2; org. phase washed (H2O), dried (Na2SO4); solvent removed; Fe complex added; dissolved in MeCN; CF3CO2H added; 25 min; DDQ added;stirred (room temp.,1 h); Et3N added; evapd. to dryness; crystd. from ethyl acetate-hexane; residue crystd. from ethyl acetate-hexane; recrystd. from THF-ethyl acetate-hexane; elem. anal.;
DOI:10.1039/b505366h