toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

Base Information

Chemical Name:toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate
CAS No.:863888-51-1
Molecular Formula:C₁₈H₂₂ClFN₂O₃
Molecular Weight:374.788
Hs Code.:

Synonyms:toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

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Chemical Property of toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

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Technology Process of toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

There total 5 articles about toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 863888-47-5
toluene-4-sulfonic acid 2-[4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)-benzyloxy]ethyl esterhexadeuterate

: 863888-51-1
toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

Guidance literature:: With potassium fluoride; [2.2.2]cryptande; In acetonitrile; at 90 ℃; for 0.166667h;

Reference yield:

: 2-tert-butyl-4-chloro-5-{4-[2-(tert-butyldimethylsilanyloxy)ethoxymethyl]benzyloxy}-2H-pyridazin-3-onehexadeuterate

: 863888-51-1
toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 20 °C / Inert atmosphere

3: potassium fluoride; [2.2.2]cryptande / acetonitrile / 0.17 h / 90 °C / Inert atmosphere

With dmap; potassium fluoride; tetrabutyl ammonium fluoride; triethylamine; [2.2.2]cryptande; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 2-tert-butyl-4-chloro-5-[4-(2-hydroxy-ethoxymethyl)benzyloxy]-2H-pyridazin-3-onehexadeuterate

: 863888-51-1
toluene-4-sulfonic acid 2-[4-(1-tertbutyl-5-chloro-6-oxo-1,6-dihydropyridazin-4-yloxymethyl)benzyloxy] ethyl ester hexadeuterate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap / dichloromethane / 20 °C / Inert atmosphere

2: potassium fluoride; [2.2.2]cryptande / acetonitrile / 0.17 h / 90 °C / Inert atmosphere

With dmap; potassium fluoride; triethylamine; [2.2.2]cryptande; In dichloromethane; acetonitrile;