6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

Base Information

Chemical Name:6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one
CAS No.:949570-80-3
Molecular Formula:C₂₀H₁₅N₃O₅
Molecular Weight:377.356
Hs Code.:

Synonyms:6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

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Chemical Property of 6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

Chemical Property:

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Technology Process of 6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

There total 9 articles about 6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949570-64-3
3-(3-methoxy-4-nitrophenyl)-6-((2-(trimethylsilyl)ethoxy)methoxy)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

: 949570-80-3
6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1021/jm070105d

Reference yield:

: 755026-96-1
2-(3-methoxy-4-nitrophenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 949570-80-3
6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Cy-MAP; CsF / Pd(OAc)2 / 1,2-dimethoxy-ethane; methanol / 12 h / Heating

2: 65 mg / aq. HCl / tetrahydrofuran; methanol / 20 °C

With hydrogenchloride; cesium fluoride; palladium diacetate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane;
DOI:10.1021/jm070105d

Reference yield:

: 949570-74-5
C₂₁H₁₇ClN₂O₅

: 949570-80-3
6-hydroxy-3-(3-methoxy-4-nitrophenyl)-5H-dibenzo[b,e][1,4]diazepin-11(10H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pt/C / methanol / 20 °C

2: TsOH*H₂O / toluene / 48 h / Heating

3: 32 percent / iPr₂NEt / CH₂Cl₂; acetonitrile / 20 °C

4: Cy-MAP; CsF / Pd(OAc)2 / 1,2-dimethoxy-ethane; methanol / 12 h / Heating

5: 65 mg / aq. HCl / tetrahydrofuran; methanol / 20 °C

With hydrogenchloride; hydrogen; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; cesium fluoride; palladium diacetate; platinum on activated charcoal; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm070105d