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Cyclohexen-(3)-yl-essigsaeure-anilid

Base Information Edit
  • Chemical Name:Cyclohexen-(3)-yl-essigsaeure-anilid
  • CAS No.:7086-69-3
  • Molecular Formula:C14H17NO
  • Molecular Weight:215.295
  • Hs Code.:
  • Mol file:7086-69-3.mol
Cyclohexen-<sup>(3)</sup>-yl-essigsaeure-anilid

Synonyms:Cyclohexen-(3)-yl-essigsaeure-anilid

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Chemical Property of Cyclohexen-(3)-yl-essigsaeure-anilid Edit
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Technology Process of Cyclohexen-(3)-yl-essigsaeure-anilid

There total 4 articles about Cyclohexen-(3)-yl-essigsaeure-anilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b00725
Guidance literature:
Multi-step reaction with 2 steps
1: dipyridinium dichromate / N,N-dimethyl-formamide / 8 h / 0 - 20 °C / Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere
With dmap; dipyridinium dichromate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.8b00725
Guidance literature:
Multi-step reaction with 3 steps
1.1: 2-methyl-but-2-ene; bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere
1.2: 12 h / 0 °C / Inert atmosphere
2.1: dipyridinium dichromate / N,N-dimethyl-formamide / 8 h / 0 - 20 °C / Inert atmosphere
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere
With dmap; dipyridinium dichromate; 2-methyl-but-2-ene; bis-(1,2-dimethylpropyl)borane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.8b00725
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