5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

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Chemical Name:5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole
CAS No.:316173-63-4
Molecular Formula:C₁₉H₂₀N₆O₂
Molecular Weight:364.407
Hs Code.:

Synonyms:5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

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Chemical Property of 5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

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Technology Process of 5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

There total 6 articles about 5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5406-18-8
3-(p-methoxyphenyl)-1-propanol

: 316173-63-4
5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

Guidance literature:: Multi-step reaction with 7 steps

1: SO₂Cl / CHCl₃ / Heating

2: 85 percent / NH₂NH₂ / ethanol / 72 h / Heating

3: 75 percent / triethylamine / ethanol / 18 h / 70 °C

4: 93 percent / 8 h / Heating

5: 2-methoxy-ethanol / 8 h / Heating

6: 4.8 g / diphenyl ether; 2-methoxy-ethanol / 1.5 h / 260 °C

7: 99 percent / aq. HCl / dioxane / 3 h / Heating

With hydrogenchloride; sulfuryl dichloride; triethylamine; hydrazine; In 1,4-dioxane; diphenylether; ethanol; chloroform; 2-methoxy-ethanol;
DOI:10.1021/jm0009843

Reference yield:

: 59623-12-0
3-(4'-methoxy phenyl)-propylchloride

: 316173-63-4
5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / NH₂NH₂ / ethanol / 72 h / Heating

2: 75 percent / triethylamine / ethanol / 18 h / 70 °C

3: 93 percent / 8 h / Heating

4: 2-methoxy-ethanol / 8 h / Heating

5: 4.8 g / diphenyl ether; 2-methoxy-ethanol / 1.5 h / 260 °C

6: 99 percent / aq. HCl / dioxane / 3 h / Heating

With hydrogenchloride; triethylamine; hydrazine; In 1,4-dioxane; diphenylether; ethanol; 2-methoxy-ethanol;
DOI:10.1021/jm0009843

Reference yield:

: 5-amino-4-cyano-1-(3-(4-methoxy)phenylpropyl)pyrazole

: 316173-63-4
5-amino-1-[3-(4-methoxy)phenylpropyl]-4-[3-(2-furyl)-1,2,4-triazol-5-yl]pyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / 8 h / Heating

2: 2-methoxy-ethanol / 8 h / Heating

3: 4.8 g / diphenyl ether; 2-methoxy-ethanol / 1.5 h / 260 °C

4: 99 percent / aq. HCl / dioxane / 3 h / Heating

With hydrogenchloride; In 1,4-dioxane; diphenylether; 2-methoxy-ethanol;
DOI:10.1021/jm0009843