(3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

Base Information

Chemical Name:(3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide
CAS No.:247233-84-7
Molecular Formula:C₄₀H₄₈I₂N₂O₁₀S
Molecular Weight:1002.7
Hs Code.:

Synonyms:(3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

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Chemical Property of (3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

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Technology Process of (3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

There total 1 articles about (3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 49617-83-6
m-Iodobenzyl bromide

: 185450-20-8
(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

: 247233-84-7
(3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm991054q

Reference yield:

: 764-48-7
ethyleneglycol vinyl ether

: 247233-84-7
(3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

: 1-{3-[(3R,4S,5S,6R)-7-(3-Acetyl-benzyl)-4,5-bis-(2-methoxy-ethoxymethoxy)-1,1-dioxo-3,6-bis-phenoxymethyl-1λ⁶-[1,2,7]thiadiazepan-2-ylmethyl]-phenyl}-ethanone

Guidance literature:: With palladium diacetate; 1,3-bis-(diphenylphosphino)propane; thallium(I) acetate; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1021/jm991054q

Reference yield:

: 3622-76-2
(2-ethenyloxyethyl)dimethylamine

: 247233-84-7
(3R,4S,5S,6R)-2,7-bis[(3-iodophenyl)methyl]-4,5-bis[(2-methoxyethoxy)methoxy]3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

: [2-((E)-2-{3-[(3R,4S,5S,6R)-7-{3-[(E)-2-(2-Dimethylamino-ethoxy)-vinyl]-benzyl}-4,5-bis-(2-methoxy-ethoxymethoxy)-1,1-dioxo-3,6-bis-phenoxymethyl-1λ⁶-[1,2,7]thiadiazepan-2-ylmethyl]-phenyl}-vinyloxy)-ethyl]-dimethyl-amine

Guidance literature:: With palladium diacetate; potassium carbonate; lithium chloride; In water; N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1021/jm991054q