3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Base Information

Chemical Name:3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol
CAS No.:470665-45-3
Molecular Formula:C₅₉H₉₀N₂O₈
Molecular Weight:955.372
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Suppliers and Price of 3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

There total 4 articles about 3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 107856-74-6
C₂₆H₅₀O₄

: 470665-43-1
2-amino-3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-1,2,5-trideoxy-D-glucitol

: 470665-45-3
3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1081/CAR-120004331

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 470665-45-3
3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Cs₂CO₃ / dimethylformamide / 16 h / 20 °C

2: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 760 Torr

3: 70 percent / (i-Pr)2NEt; PyBOP / CH₂Cl₂

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120004331

Reference yield:

: 250737-19-0
3,4,6-tri-O-benzyl-2-[(benzyloxycarbonyl)amino]-1,2,5-trideoxy-1,5-imino-D-glucitol

: 470665-45-3
3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-[(R)-3-(dodecanoyloxytetradecanoyl)]amino-1,2,5-trideoxy-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Cs₂CO₃ / dimethylformamide / 16 h / 20 °C

2: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 760 Torr

3: 70 percent / (i-Pr)2NEt; PyBOP / CH₂Cl₂

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120004331