2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

Base Information

Chemical Name:2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin
CAS No.:668441-11-0
Molecular Formula:C₁₆H₂₀O₃S₂
Molecular Weight:324.465
Hs Code.:

Synonyms:2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

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Chemical Property of 2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

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Technology Process of 2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

There total 2 articles about 2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35756-26-4
2,3-dihydro-5-phenyl-1,4-dithiin

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 668441-11-0
2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

: 2-phenyl-3-[(1'R,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

Guidance literature:: With titanium(IV) isopropylate; n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, hexane, -78 deg C, 2.) THF, hexane, a) -78 deg C, 30 min, b) -20 deg C, overnight;
DOI:10.1016/0040-4020(96)00677-1

Reference yield:

: C₁₀H₉LiS₂

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 668441-11-0
2-phenyl-3-[(1'S,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

: 2-phenyl-3-[(1'R,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

Guidance literature:: With titanium(IV) isopropylate; In tetrahydrofuran; hexane; at -78 - -20 ℃; Product distribution; Mechanism; other chiral aldehydes; var. catalysts;
DOI:10.1016/0040-4020(96)00677-1