N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

Base Information

Chemical Name:N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide
CAS No.:676147-57-2
Molecular Formula:C₁₆H₁₈N₂O₄S
Molecular Weight:334.396
Hs Code.:

Synonyms:N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

Suppliers and Price of N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

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Technology Process of N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

There total 1 articles about N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 676147-57-2
N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

Guidance literature:: In ethanol; at 20 ℃; for 2h;

Reference yield: 92.0%

: 661-68-7
1,2-difluoro-1,1,2,2-tetramethyl-disilane

: 676147-57-2
N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

: ((3,5-dimethoxyphenyl)methylene)bis(fluorodimethylsilane)

Guidance literature:: With bis(dibenzylideneacetone)-palladium⁽⁰⁾; lithium tert-butoxide; ethriol phosphite; In toluene; at 60 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.5b09135

Reference yield: 79.0%

: 676147-57-2
N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide

: 3-bromo-N-(2-nitrophenyl)pyridin-2-amine

: 2-(3-(3,5-dimethoxyphenyl)-1H-pyrrolo[2,3-b]pyridin-1-yl)aniline

Guidance literature:: N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonylhydrazide; 3-bromo-N-(2-nitrophenyl)pyridin-2-amine; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; XPhos; In 1,4-dioxane; at 20 ℃; for 0.0166667h; Sealed tube; Inert atmosphere;

With lithium tert-butoxide; In 1,4-dioxane; at 110 ℃; for 5h; Sealed tube; Inert atmosphere;

With triphenylphosphine; In 1,4-dioxane; at 160 ℃; for 24h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.7b03422