C₃₉H₄₈O₁₃

Base Information

Chemical Name:C₃₉H₄₈O₁₃
CAS No.:1369430-79-4
Molecular Formula:C₃₉H₄₈O₁₃
Molecular Weight:724.802
Hs Code.:

C<sub>39</sub>H<sub>48</sub>O<sub>13</sub>

Synonyms:C₃₉H₄₈O₁₃

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Chemical Property of C₃₉H₄₈O₁₃

Chemical Property:

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Technology Process of C₃₉H₄₈O₁₃

There total 21 articles about C₃₉H₄₈O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 10276-09-2
2,2-dimethyl-but-3-enoic acid

: 1240304-31-7
(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

: 1369430-79-4
C₃₉H₄₈O₁₃

Guidance literature:: With triethylamine; palladium diacetate; tris-(o-tolyl)phosphine; In acetonitrile; for 3h; Inert atmosphere; Reflux;

Reference yield:

: 1240304-54-4
1,5-dibromo-2-(methoxymethoxy)-4-(propan-2-yl)benzene

: 1369430-79-4
C₃₉H₄₈O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.92 h / -86 - -74 °C / Inert atmosphere

1.2: 1.47 h / -86 - -74 °C

2.1: methanesulfonic acid / methanol / 1 h / Reflux

3.1: acetic anhydride; N-ethyl-N,N-diisopropylamine / dmap / tetrahydrofuran / 21 h / 20 °C

4.1: trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane / water; acetonitrile / 1.5 h / Cooling

4.2: 0.42 h / Cooling

5.1: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 3 h / Inert atmosphere; Reflux

With n-butyllithium; methanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane; acetic anhydride; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; hexane; water; acetonitrile; 5.1: Heck Reaction;

Reference yield:

: 1017608-23-9
2-iodo-5-(propan-2-yl)phenol

: 1369430-79-4
C₃₉H₄₈O₁₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: potassium carbonate / acetonitrile / 2 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

2.2: 0.58 h / -78 °C

3.1: methanesulfonic acid / methanol / 14.5 h / 20 °C

4.1: pyridine; acetic anhydride / dmap / 19 h / 4 - 20 °C

5.1: triethylsilane; boron trifluoride diethyl etherate / chloroform; acetonitrile / 1.5 h / 4 °C / Inert atmosphere

6.1: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C

7.1: bromine / acetic acid / 20 °C

8.1: water; triethylamine / methanol / 25 h / 20 - 50 °C

9.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 1 h / 4 °C / Inert atmosphere

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

10.2: 1 h / -78 °C

11.1: methanesulfonic acid / methanol / 0.5 h / 20 °C

12.1: pyridine; acetic anhydride / dmap / 30 h / 20 °C

13.1: triethylsilane; boron trifluoride diethyl etherate / chloroform; acetonitrile / 0.5 h / 4 - 20 °C / Inert atmosphere

14.1: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 3 h / Inert atmosphere; Reflux

With pyridine; triethylsilane; n-butyllithium; chloro-trimethyl-silane; methanesulfonic acid; boron trifluoride diethyl etherate; water; hydrogen; bromine; acetic anhydride; potassium carbonate; triethylamine; dmap; palladium on activated charcoal; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; hexane; chloroform; acetic acid; N,N-dimethyl-formamide; acetonitrile; 14.1: Heck Reaction;