Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide

Base Information

• Chemical Name: Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide
• CAS No.: 126046-20-6
• Molecular Formula: BrH*C₁₆H₁₅N₃O₃
• Molecular Weight: 378.225

Synonyms:Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide

Chemical Property of Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide

Chemical Property:

Purity/Quality:

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Technology Process of Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide

There total 2 articles about Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-({[2-Oxo-2-(4-phenylazo-phenyl)-ethoxycarbonylmethyl]-amino}-methylene)-malonic acid diethyl ester (126046-05-7) → Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide (126046-20-6)

Guidance literature:

With bromine; In chloroform; Ambient temperature;

DOI:10.1055/s-1989-27312

Reference yield:

4-(Phenylazo)phenacyl bromide (62625-24-5) → Amino-acetic acid 2-oxo-2-(4-phenylazo-phenyl)-ethyl ester; hydrobromide (126046-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / Et₃N / acetone / 0.5 h / Ambient temperature

2: 85 percent / 4percent Br₂ / CHCl₃ / Ambient temperature

With bromine; triethylamine; In chloroform; acetone;

DOI:10.1055/s-1989-27312

upstream raw materials:

2-({[2-Oxo-2-(4-phenylazo-phenyl)-ethoxycarbonylmethyl]-amino}-methylene)-malonic acid diethyl ester

4-(Phenylazo)phenacyl bromide

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