cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

Base Information

Chemical Name:cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate
CAS No.:1018674-58-2
Molecular Formula:C₂₆H₄₁N₃O₅
Molecular Weight:475.629
Hs Code.:

Synonyms:cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

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Chemical Property of cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

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Technology Process of cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

There total 8 articles about cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1018674-57-1
1-benzyl 2-cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-1,2-dicarboxylate

: 1018674-58-2
cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

Guidance literature:: With hydrogen; palladium dihydroxide; In ethyl acetate; for 1h;

Reference yield:

: 56703-34-5
3-[4-(hydroxymethyl)phenyl]propanoic acid

: 1018674-58-2
cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: manganese(IV) oxide / dichloromethane / 18 h / 35 °C

2: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 18 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 21 h / 20 - 50 °C

4: hydrogen / palladium dihydroxide / ethyl acetate / 1 h

With manganese(IV) oxide; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium dihydroxide; In dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 283153-64-0
methyl 3-(4-(hydroxymethyl)phenyl)propanoate

: 1018674-58-2
cyclopentyl 4-(4-{3-[(1-isobutoxyethoxy)amino]-3-oxopropyl}benzyl)piperazine-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide / methanol; water / 18 h / 20 °C

1.2: pH 3

2.1: manganese(IV) oxide / dichloromethane / 18 h / 35 °C

3.1: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 18 h / 20 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 21 h / 20 - 50 °C

5.1: hydrogen / palladium dihydroxide / ethyl acetate / 1 h

With manganese(IV) oxide; lithium hydroxide; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium dihydroxide; In methanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;