NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

Base Information

Chemical Name:NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)
CAS No.:90413-02-8
Molecular Formula:C₃₃H₃₁NiOP₃S₃
Molecular Weight:691.418
Hs Code.:

NiS<sub>3</sub>P(C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)2(CH<sub>2</sub>)2P(C<sub>6</sub>H<sub>5</sub>)2)

Synonyms:NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

Suppliers and Price of NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

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Chemical Property of NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

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Technology Process of NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

There total 2 articles about NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 14647-23-5
1,2-bis(diphenylphosphino)ethane nickel(II) chloride

: 90432-13-6
(CH₃C₅H₄)2TiS₄P₂(C₆H₄OCH₃)2

: 1282-40-2
dichlorobis(η5-methylcyclopentadienyl)titanium(IV)

: 90413-02-8
NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

Guidance literature:: In tetrahydrofuran; byproducts: (C6H4OCH3PS)3; The soln. of reagents in THF was stirred for 20 h (N2 atm.);; evapd., recrystd. by dilution of CH2Cl2 soln. with methanol; elem. anal.;;

Reference yield: 83.0%

: 14647-23-5
1,2-bis(diphenylphosphino)ethane nickel(II) chloride

: 90412-94-5
2Li⁽¹⁺⁾*S₃PC₆H₄OCH₃^(2-)

: 90413-02-8
NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

Guidance literature:: In tetrahydrofuran; The THF- soln. of reagents was stirred for 2 h (N2 atm.);; evapd., extd. with CH2Cl2, MeOH was added, concd., cooled to -25°C; filtered, washed with cold MeOH; elem. anal.;;

Reference yield: 91.0%

: 421-20-5
Methyl fluorosulfonate

: ammonium hexafluorophosphate

: 90413-02-8
NiS₃P(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)

: 90413-04-0
NiS₂P(SCH₃)(C₆H₄OCH₃)(P(C₆H₅)2(CH₂)2P(C₆H₅)2)⁽¹⁺⁾*PF₆^(1-)

Guidance literature:: In dichloromethane; A CH2Cl2 soln. of complex and FSO3Me was stirred for 4 h, evapd., MeOH was added, MeOH-soln. of NH4PF6 was added, the soln. was stirred for 3 h(N2 atm.);; concd., cooled to -25°C, filtered, washed with cold MeOH; elem. anal.;;